High-performance liquid chromatography with tandem mass spectrometry method for the determination of norcantharidin in human serum

• In: SIG Bioavailability/Bioequivalence - Posters
• At: Beijing (China) (2007)
• Type: Poster
• Poster code: BB-P-036
• By: WEI, Chunmin (Qilu Hospital, Jinan, China)
• Co-author(s): WANG, Ben-jie (Qilu Hospital, JINAN, China)
  ZHANG, Rui (Qilu Hospital, JINAN, China)
  GAO, Yan-hui (Shandong University, JINAN, China)
  
• Abstract:

  OBJECTIVE A sensitive, simple and selective high-performance liquid chromatography -tandem mass spectrometry (HPLC-MS-MS) method was developed and applied to the determination of norcantharidin concentration in human serum. METHODS Norcantharidin and cyclophosphamide as internal standard (I.S.) in serum were extracted with acetone, separated on a..

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