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Robustness of RP-HPLC method for the determination of valdecoxib and its impurity SC-77852

  • At: 2006 FIP Congress in Salvadore (Brazil)
  • Type: Poster
  • By: ZECEVIC, Mira (Faculty of Pharmacy, Belgrade, Belgrade, Yugoslavia)
  • Co-author(s): Savic, Gordana (Medicines and Medical Devices Agency of, BELGRADE, Serbia and Montenegro)
    Zivanovic, Ljiljana (Faculty of Pharmacy, Belgrade, BELGRADE, Serbia and Montenegro)
  • Abstract:

    A reversed-phase liquid chromatography method was developed and validated for the evaluation of valdecoxib and impurity SC-77852, which constitutes of a–N-lactosyl sulfonamide and ß–N-lactosyl sulfonamide, i.e. a and ß-anomer. The separation is achieved on monolithic HPLC column. Presented RP-HPLC method is fully validated for its linearity,

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Last update 4 October 2019

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