Synthesis of pyrazoloisoquinolines as chemiluminescence luminol precursors

  • At: 2017 FIP Congress in Seoul (South Korea)
  • Type: Poster
  • By: TSAI, Shuo-En (China Medical University, Taichung City, China Taiwan)
  • Co-author(s): Shuo-En Tsai: School of Pharmacy, China Medical University, Taichung City, Taiwan, Province of China
    Wan-Ping Yen: School of Pharmacy, China Medical University, Taichung City, Taiwan, Province of China
    Fung-Fuh Wong: School of Pharmacy, China Medical University, Taichung City, Taiwan, Province of China
  • Abstract:

    Methods

    A sealable oven-dried tubular reaction vessel was charged with N,N-diisopropylamidinyl pyrazoylimines , diethyl acetylenedicarboxylate in the presence of various metal catalysts in various solvents at ~80–90 °C within 24 h under the nitrogen atmosphere.

    When the reaction was completed, the reaction mixture was filtered to remove metal

    ..

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